An Efficient Method for the Preparation of Sulfonyl Chlorides: Reaction of Disulfides or Thiols with Sodium Hypochlorite Pentahydrate (NaOCl·5H2O) Crystals

Tomohide Okada,Hiroaki Matsumuro,Toshiaki Iwai,Saori Kitagawa,Kento Yamazaki,Tomomi Akiyama,Tomotake Asawa,Yukihiro Sugiyama,Yoshikazu Kimura,Masayuki Kirihara

An Efficient Method for the Preparation of Sulfonyl Chlorides: Reaction of Disulfides or Thiols with Sodium Hypochlorite Pentahydrate (NaOCl·5H2O) Crystals

2015

Tomohide Okada
Hiroaki Matsumuro
Toshiaki Iwai
Saori Kitagawa
Kento Yamazaki
Tomomi Akiyama
Tomotake Asawa
Yukihiro Sugiyama
Yoshikazu Kimura
Masayuki Kirihara

The reaction of disulfides or thiols with sodium hypochlorite pentahydrate in acetic acid efficiently provided the corresponding sulfonyl chlorides in high yields.

Keywords:

Sodium hypochlorite
Sulfonyl
Crystal
Chemistry
Organic chemistry
Acetic acid

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