Integration of Multi-Scale 3D Imaging of Porosity in Shales

In this research the Haynesville-Bossier Shale play (USA), which is a clay-bearing siliceous, organic-rich, gas-mature shale play, was characterized over pore diameters ranging 2 nm to 3000 nm. Three advanced imaging techniques were utilized correlatively, including the application of Xe plasma focused ion beam scanning electron microscopy (plasma FIB or PFIB), complemented by the Ga FIB method which is now frequently used to characterise porosity and organic/inorganic phases, together with transmission electron microscope tomography of the nano-scale pores. This is the first study to comprehensively develop pore geometric and network models in 3D based on experimental characterisation over these critical length scales