Phthalide synthesis through dehydrogenated lactonization of the C(sp3)–H bond by photoredox catalysis
2021
A practical and efficient method is established for the direct oxidative lactonization of the C(sp3)–H bonds relying on visible-light-induced photoredox catalysis. This protocol expediently allows the delivery of diverse phthalides using oxygen as the sole terminal oxidant under metal-free conditions at room temperature. Notably, the choice of an appropriate hydrogen atom transfer (HAT) cocatalyst is revealed to be critical for the success of this process.
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