Scalable On-Demand Production of Purified Diazomethane Suitable for Sensitive Catalytic Reactions

We have developed a convenient development-scale reactor (0.44 mol/h) to prepare diazomethane from N-methyl-N-nitroso-p-toluenesulfonamide (MNTS) in ∼80% yield. Diazomethane (CH2N2) made with this ...