Synthesis of structurally diverse diarylketones through the diarylmethyl sp3 CH oxidation
2014
Abstract Under open-flask conditions, an efficient method to assemble a series of diversely functionalized diarylketones in the presence of commercially available NBS has been developed. Yields of up to 99% have been achieved employing diarylmethanes as starting material. Based on 18 O-labeled experiment, the addition of stoichiometric water eventually leads to excellent yields in all carbonylation cases.
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