An Analysis of Microstructures Properties and Failure Process Based on Mafic Specimens under Compressive Tests and Quantitative Scanning Electron Microscope Images Processing

2020 
Abstract The micro-structures of rock govern meso- and macro-scale rock behaviours and their failure mechanisms. This paper applied the experimental study (uniaxial and triaxial compressive tests) and scanning electron microscope (SEM) method to illustrate the relationship between microscopic damage and mesoscopic fracture. Specifically, this study carried out that there are three main pre-existing micro-structures including heterogeneity (31%), micro-cracks (27%), and crystal lattice boundaries (25%). The pre-existing micro-cracks are investigated and classified as inter-granular cracks (37%), intra-granular cracks (36%), and trans-granular cracks (27%) based on morphological characteristics. According to the deformation types, the micro-cracks after test are divided as tensile crack (53%), shear crack (29%), and mixed shear and tensile crack (18%). Moreover, this paper provides a damage property parameter which is the ratio of tensile damage degree to shear damage degree based on the SEM image processing technique. This parameter could reveal the damage properties (tensile or shear) at different stages including initiating stage, propagation stage and failure stage, which could present the microscopic damage development process. Finally, compared with the fractures on two specimens from compressive tests, it could confirm that the meso-scale fracturing process is associated with the micro-scale damage development process.
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