Synthesis of a linearly linked triscalixarene consisting of calix[4]arene units with combined axial chirality and inherent chirality
2017
A linearly linked triscalix[4]arene, in which each calix[4]arene unit possesses both axial chirality and inherent chirality, was synthesized by repeated use of two stereoselective Williamson etherification on calix[4]arene. In the crystal lattice of the biscalix[4]arene intermediate, there are interesting alternate layers of biscalixarene molecules and solvent molecules in the ab plane.
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