Heat flow reaction calorimetry under reflux conditions
1993
Abstract A brief review of the procedures used in heat flow reaction calorimetry experiments under reflux and their evaluation is presented. A method to calibrate global heat transfer coefficients and the mass flow of the cooling condenser fluid under refluxing conditions is validated and discussed through experiments with pure solvents. A study of the influence of the most significant experimental conditions on the accuracy of the measurements is also considered.
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