Tris(4‐bromophenyl)aminium Hexachloroantimonate
2011
[24964-91-8] C18H12Br3Cl6NSb (MW 816.46)
InChI = 1/C18H12Br3N.6ClH.Sb/c19-13-1-7-16(8-2-13)22(17-9-3-14(20)4-10-17)18-11-5-15(21)6-12-18;;;;;;;/h1-12H;6*1H;/q+1;;;;;;;+5/p-6/fC18H12Br3N.6Cl.Sb/h;6*1h;/qm;6*-1;m/rC18H12Br3N.Cl6Sb/c19-13-1-7-16(8-2-13)22(17-9-3-14(20)4-10-17)18-11-5-15(21)6-12-18;1-
InChIKey = SDHBPVANTRLAKE-GPPCHKDRCL
(a stable radical cation2 and one-electron oxidant2)
Physical Data: mp 142 °C.2
Solubility: sol acetonitrile, dichloromethane.
Form Supplied in: dark blue crystalline solid.
Purification: one method is as follows: a solution of the title reagent 1 in dichloromethane (1 part) is poured into diethyl ether (3 parts) to precipitate the salt; the resulting blue needles are collected and dried under vacuum.2
Handling, Storage, and Precautions: is an irritant and is moisture sensitive.
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KQI